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Elements of Chemistry

Page 267 of 329, printed 267

is necessary in adapting bent tubes to the necks of bottles in the apparatus represented Pl. IV. Fig. 1. and others of a similar nature. Each mouth of each bottle must be fitted with a cork, having a hole made with a round file of a proper size for containing the tube. And, when one mouth is intended to admit two or more tubes, which frequently happens when we have not a sufficient number of bottles with two or three necks, we must use a cork with two or three holes, Pl. IV. Fig. 8. When the whole apparatus is thus solidly joined, so that no part can play upon another, we begin to lute. The lute is softened by kneading and rolling it between the fingers, with the assistance of heat, if necessary. It is rolled into little cylindrical pieces, and applied to the junctures, taking great care to make it apply close, and adhere firmly, in every part; a second roll is applied over the first, so as to pass it on each side, and so on till each juncture be sufficiently covered; after this, the slips of bladder, or of linen, as above directed, must be carefully applied over all. Though this operation may appear extremely simple, yet it requires peculiar delicacy and management; great care must be taken not to disturb one juncture whilst luting another, and more especially when applying the fillets and ligatures. Before beginning any experiment, the closeness of the luting ought always to be previously tried, either by slightly heating the retort A, Pl. IV. Fig. 1, or by blowing in a little air by some of the perpendicular tubes S s s s; the alteration of pressure causes a change in the level of the liquid in these tubes. If the apparatus be accurately luted, this alteration of level will be permanent; whereas, if there be the smallest, opening in any of the junctures, the liquid will very soon recover its former level. It must always be remembered, that the whole success of experiments in modern chemistry depends upon the exactness of this operation, which therefore requires the utmost patience, and most attentive accuracy. It would be of infinite service to enable chemists, especially those who are engaged in pneumatic processes, to dispense with the use of lutes, or at least to diminish the number necessary in complicated instruments. I once thought of having my apparatus constructed so as to unite in all its parts by fitting with emery, in the way of bottles with cristal stoppers; but the execution of this plan was extremely difficult. I have 267
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